Title
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Microstructure and precipitates in annealed ferromagnetic shape memory alloy
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Author
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Abstract
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Transmission electron microscopy was performed to investigate the microstructure and precipitates in the annealed Co38Ni33Al29 ferromagnetic shape memory alloy. Apart from the dendritic secondary phase in the austenite matrix, micron-sized (up to 100 μm) fcc-based precipitates with partial γ′ L12 ordering and containing none, one or three {1 1 1}p parallel twin planes were found. The orientation relationship between the precipitates and matrix was found to be KurdjumovSachs. STEMEDX analysis indicates that twinned and non-twinned precipitates are Co-rich and Al- and Ni-deficient with respect to the matrix and with a lower Co/Al ratio for the latter. The 3D morphologies of precipitates were reconstructed with focused ion beam/scanning electron microscope dual-beam slice-and-view imaging, showing that the single {1 1 1}p plane twinned precipitates have a plate-like shape while the non-twinned precipitates are lath-like and often bent. |
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Language
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English
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Source (journal)
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Journal of alloys and compounds. - Amsterdam
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Publication
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Amsterdam
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2013
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ISSN
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0925-8388
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DOI
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10.1016/J.JALLCOM.2013.03.228
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Volume/pages
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572
(2013)
, p. 5-10
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ISI
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000319209600002
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Full text (Publisher's DOI)
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Full text (publisher's version - intranet only)
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