Title
Evaluation of pulsed radiofrequency glow discharge time-of-flight mass spectrometry for precious metal determination in lead fire assay buttons Evaluation of pulsed radiofrequency glow discharge time-of-flight mass spectrometry for precious metal determination in lead fire assay buttons
Author
Faculty/Department
Faculty of Applied Engineering Sciences
Publication type
article
Publication
Amsterdam ,
Subject
Chemistry
Engineering sciences. Technology
Source (journal)
Analytica chimica acta. - Amsterdam
Volume/pages
701(2011) :2 , p. 129-133
ISSN
0003-2670
ISI
000294144400002
Carrier
E
Target language
English (eng)
Full text (Publishers DOI)
Abstract
In this paper, an exploration of the capabilities and limitations of pulsed radiofrequency glow discharge time-of-flight mass spectrometry (GD-TOFMS) for the determination of the precious metals Ag, Au, Pd, Pt and Rh in lead buttons obtained by Pb fire assay is reported on. Since the matrix consists almost entirely of lead (>99%), the occurrence of doubly charged Pb (Pb2+) ions...
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