Title
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Quaternary (M = Ni, Zn, Co, Mn) ferrite oxides : synthesis, characterization and magnetic properties
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Author
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Abstract
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We report the synthesis of M0.25Cu0.25Mg0.5Fe2O4 (where M = Mn, Zn, Co, Ni) nanoparticles using the coprecipitation method in the presence of carboxymethyl cellulose (CMC) as the in-situ surfactant. The crystalline structure and surface morphology were examined by means of X-ray diffraction (XRD) and scanning electron microscopy (SEM) and it was established that the average diameter of the magnetic nanoparticles (MNPs) is in the range of 310 nm. X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR) show that the MNPs are activated by the hydrophilic groups of the surfactant, which coat them and enhance their stability. The vibrating sample magnetometry measurements show the superparamagnetic behavior of the nanoparticles. Due to their small crystallite size, which implies large surface area, and their functionalization with organic groups, the obtained nanoparticles could have medical and catalytic applications. |
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Language
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English
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Source (journal)
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Materials research bulletin. - New York, N.Y.
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Publication
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New York, N.Y.
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2016
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ISSN
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0025-5408
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DOI
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10.1016/J.MATERRESBULL.2016.05.001
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Volume/pages
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81
(2016)
, p. 63-70
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ISI
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000379558100009
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Full text (Publisher's DOI)
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Full text (open access)
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Full text (publisher's version - intranet only)
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