Title
Electron microscopy and X-ray study of the growth of <tex>$FeCr_{2}S_{4}$</tex> spinel single crystals by chemical vapour transport Electron microscopy and X-ray study of the growth of <tex>$FeCr_{2}S_{4}$</tex> spinel single crystals by chemical vapour transport
Author
Faculty/Department
Faculty of Sciences. Physics
Publication type
article
Publication
Berlin ,
Subject
Chemistry
Source (journal)
Crystal research and technology. - Berlin
Volume/pages
28(1993) :8 , p. 1051-1061
ISSN
0232-1300
ISI
A1993MN86700003
Carrier
E
Target language
English (eng)
Full text (Publishers DOI)
Affiliation
University of Antwerp
Abstract
The growth features of FeCr2S4 spinel single crystals prepared by chemical vapour transport were studied by means of scanning electron microscopy, transmission electron microscopy, high resolution electron microscopy, electron diffraction and X-ray analysis. Our results indicate that the epitaxial growth of the new phases FeCr7S12 and FeCr8S12, both based on the NiAs structure, can essentially inhibit the growth of large FeCr2S4 spinel single crystals in the octahedral habit. The new phases are fully characterised and the effects of defect ordering in these new phases are also reported.
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