|
Title
|
|
|
|
Revealing nanoscale structural TEM/HRTEM: application on ferroelectric ordering by PMN-PT relaxor ferroelectric
| |
|
Author
|
|
|
|
| |
|
Abstract
|
|
|
|
| Nano-scale ordering may be revealed in transmission electron microscopy (TEM) by at least three techniques that will be presented in this work: selected area electron diffraction, conventional TEM and high-resolution TEM. Digital image processing is used to extract additional information from the high-resolution micrographs. The described methods are illustrated in a microstructural and compositional study of a 90%Pb(Mg1/3Nb2/3)O-3-10%PbTiO2 ceramic sample. High-resolution images reveal the presence of ordered compositional nano-domains, observable in two specific crystallographic orientations. Antiphase boundaries lying in the (111) planes separate them, while (100) and (111) facets separate the ordered domains from the disordered matrix. |
| |
|
Language
|
|
|
|
English
| |
|
Source (journal)
|
|
|
|
Journal of optoelectronics and advanced materials. - Bucharest
| |
|
Publication
|
|
|
|
Bucharest
:
2008
| |
|
ISSN
|
|
|
|
1454-4164
| |
|
Volume/pages
|
|
|
|
10
:9
(2008)
, p. 2328-2333
| |
|
ISI
|
|
|
|
000259590400029
| |
|