Title
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Combined SEM/EDX and micro-Raman spectroscopy analysis of uranium minerals from a former uranium mine
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Author
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Abstract
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Samples of the secondary uranium minerals collected in the abandoned uranium mine at Pecs (Hungary) were investigated by two micro-techniques: scanning electron microscopy (SEM/EDX) and micro-Raman spectroscopy (MRS). They were applied to locate U-rich particles and identify the chemical form and oxidation state of the uranium compounds. The most abundant mineral was a K and/or Na uranyl sulphate (zippeite group). U(VI) was also present in the form showing intensive Raman scattering at 860 cm−1 which can be attributed to uranium trioxide. This research has shown the successful application of micro-Raman spectroscopy for the identification of uranyl mineral species on the level of individual particles. |
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Language
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English
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Source (journal)
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Journal of hazardous materials. - Amsterdam
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Publication
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Amsterdam
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2009
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ISSN
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0304-3894
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Volume/pages
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168
:1
(2009)
, p. 416-423
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ISI
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000267567600060
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Full text (Publisher's DOI)
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