Title
Molecular and crystal structures of <tex>$Cp^{*}M(S_{2}N_{2})$</tex> (M = Co, Rh, Ir) and related compounds Molecular and crystal structures of <tex>$Cp^{*}M(S_{2}N_{2})$</tex> (M = Co, Rh, Ir) and related compounds
Author
Faculty/Department
Faculty of Sciences. Chemistry
Publication type
article
Publication
Weinheim ,
Subject
Chemistry
Source (journal)
European journal of inorganic chemistry. - Weinheim
Volume/pages
(2009) :29/30 , p. 4483-4490
ISSN
1434-1948
ISI
000271572100015
Carrier
E
Target language
English (eng)
Full text (Publishers DOI)
Affiliation
University of Antwerp
Abstract
Cp*Rh(S2N2) was prepared as a microcrystalline solid by using [S4N3]Cl in liquid ammonia or [nBu2Sn(S2N2)]2. It was characterised by NMR, IR and Raman spectroscopy andmass spectrometry. Low-temperature crystal structures of Cp*Co(S2N2) and Cp*Ir(S2N2) were determined. The experimental characterisation of the Cp*M(S2N2) complexes was complemented by calculated geometries and bond orders at the DFT/B1B95 level of theory.
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