Title
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Non-destructive characterization of CoTSPc electrochemically deposited on gold electrodes by means of synchrotron X-ray microfluorescence
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Author
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Abstract
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This paper gives a detailed study of the morphology and heterogeneity of an electrodeposited cobalt tetrasulphophthalocyanine tetrasodium salt (Co(II)TSPc) layer. A continuous potential cycling of the electrode between two potentials can lead to a modification of a bare electrode. During the modification, a non-destructive characterization by means of scanning synchrotron X-ray fluorescence radiation has been made as a function of scan number. Moreover, electrochemical and SR-XRF measurements were performed in order to calculate the adsorbed Co surface concentration and to distinguish between monomer and dimer adsorption. |
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Language
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English
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Source (journal)
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Electrochemistry communications. - Amsterdam
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Publication
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Amsterdam
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2005
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ISSN
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1388-2481
1873-1902
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DOI
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10.1016/J.ELECOM.2005.08.015
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Volume/pages
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7
:11
(2005)
, p. 1157-1162
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ISI
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000232995700015
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Full text (Publisher's DOI)
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